Posts Tagged ‘Solvent Extraction’
Obtaining odorants – expression May 22, 2009 | 12:03 pm

Odorants are a very important factor in the creation of perfumes. They are basically obtained by drawing out aromatic compounds from suitable raw materials which are obtained from parts of the plant or other natural sources. Although they can be created through synthetic methods too, the natural methods used in extraction of essential oils are far more superior and in demand. The whole procedure of extraction of odorants requires it to go through several processes.
There are different methods employed for the extraction of essential oils from natural sources, like distillation, solvent extraction, expression, enfleurage, etc. The method used depends upon the nature of the raw materials. These processes results in end products like essential oils, absolutes, concretes, or butters according to the wax concentrate on the extract.

Expression is one such process employed in the extraction of aromatic compounds. In this method, the raw materials used are squeezed, pressed, or compressed to extract the oil from it. This is a technique which is frequently employed in the extraction of oils from fruit peels, especially of those which fall into the category of the citrus family. The peels from such fruits contain a large amount of oil and hence expression is one method where all the oil can be taken out in the most economically viable manner. Normally, the peels are cold pressed or expressed mechanically for the maximum benefit.

Expression, as a method of extraction is a comparatively low cost method and when combined with the easy availability of raw materials, it is generally seen that citrus oils are cheaper in the market than other aromatic oils. Examples of such oils are lemon and sweet orange oils that are among the low cost oils in the aromatic industry.

The method of expression has been in use since very ancient times, as can be found in traditional Egyptian practices. It came into the picture long before distillation. Conventionally, the ancient Egyptians used to press the raw plant material and bury it in the dessert for a few months in unglazed ceramic utensils to dry out the water content which naturally used to get diffused through the pores of the ceramic vessel. What would remain inside the pot was the oil, which used to be taken out. It can be seen that scents obtained in such a manner still managed to retain its fragrance even after 3000 years, as can be proved from the lotus oil found in sealed alabaster vessels which were found in Tutankhamen’s tomb.

Tim Walt

Obtaining odorants – Maceration April 28, 2009 | 06:21 pm

Before the creation of perfumes it is essential to obtain odorants to be used in the various process of its composition. Odorants can be obtained through synthetic as well as natural methods. While synthetically, odorants are produced through organic synthesis and purification, natural methods of extraction vary according to the type of plant as well as the type of oil that is produced. Every method adopted does not give equal results and the degree and quality of the essential oil obtained out of the different processes will differ. It should be remembered that as the difficulty of the process increases, the purity of the oil will be more and so will the expense. The cheaper methods employed may sometimes cause allergies in the skin.

Maceration is one of the most frequently used technique in the extraction of essential oils and it is also considered economical too. As a result this technique is widely used for extraction in the perfume industry today. Also known as solvent extraction, the process employed in this method is quite simple. Maceration makes use of a solvent which has the power to dissolve the desired aromatic compounds. The required raw materials are submerged in this solvent to obtain the desired results.

The duration of dissolving the raw materials in the solvent and extraction of aromatic compounds may take anywhere from a couple of hours to months together. It depends upon the material that is immersed and the quality of the essential oil that has to be extracted. Some of the main oils extracted this way are those obtained from woody and fibrous plant materials as well as those obtained from animal sources.

The method of maceration or solvent extraction is also employed in such cases where the odorants are extremely volatile or highly denatured due to heat. The process of maceration is gentle enough then to deliver high quality aromatic oil safely.

The process of maceration makes use of several suitable solvents for achieving the purpose. The most common among the solvents used in this process are hexane, ethanol, and di methyl ether. The name given for the product obtained after the process of maceration is ‘Concrete’.

Tim Walt